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Beilstein J. Org. Chem. 2016, 12, 154–165, doi:10.3762/bjoc.12.17
Graphical Abstract
Scheme 1: Synthesis of 1-4; only the isolated and characterized complexes are shown.
Figure 1: Solid state structure of complexes 2a and 2b as retrieved from single crystal X-ray diffraction.
Figure 2: Time/conversion plot for the polymerization of 5 by preinitiators 1–4 in the presence of HCl ([5]:[...
Figure 3: 1H NMR spectrum in the low-field region of the active species for complexes 4 and M32.
Scheme 2: Energetics of 2a and 2b protonation in kcal/mol.
Figure 4: Reaction pathway of the transformation of 2b to HovII (energies in kcal/mol; main distances in Å).
Figure 5: DTA-TGA measurements for polymerizations of DCPD with catalysts 1b and 2b; Reaction conditions: [ca...
Beilstein J. Org. Chem. 2010, 6, 1091–1098, doi:10.3762/bjoc.6.125
Figure 1: General layout for modifications of ruthenium-based olefin metathesis catalysts (red: anionic ligan...
Scheme 1: Synthesis of 1, 2 and 3.
Figure 2: Details of the 1H NMR spectra acquired during the synthesis of 2 and the FD-MS spectrum of 2 isolat...
Figure 3: ORTEP drawing of 3. Thermal ellipsoids are drawn at 50% probability level. Hydrogen atoms are omitt...
Figure 4: Polymerisation of 4 as a function of time, initiated by 1, 2 or 3, monitored by 1H NMR spectroscopy...
Figure 5: Polymerisations of 6 as a function of time, initiated by 1–3, monitored by 1H NMR spectroscopy (sol...
Figure 6: The RCM reaction of 7 as a function of time, catalysed by 1, 2 or 3, monitored by 1H NMR spectrosco...